HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19822236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | HCID 19822248 | HCID 19822248 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19822236 | HCID 19822236 | — |
Reaction Steps
Following the same procedure as described in Preparation 18, 3.4 g of 6-acetoxy-2-(4-aminophenoxymethyl)-2-hydroxy-5,7,8-trimethylchroman-4-one (prepared as described in Preparation 44), 40 ml of acetone, 5 ml of 35% w/v aqueous hydrochloric acid, 1.2 g of sodium nitrite, 1.6 ml of water, 13 g of ethyl acrylate and 0.32 g of cuprous oxide were reacted, to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104888 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-91513605f0cd40b888afac0097e68913 |
| Source note | uspto-grants-1992_04 |