反应详情

To a solution of 6.8M NaOH 15.8 g (0.076 mol) of 2,3-diacetamidophenol was added and the mixture was heated under reflux for 2 h. Upon cooling the pH of the solution was adjusted to 8.5 with 2M HCl. The solid was filtered off, washed with water and dried to give 7.6 g of the title compound.

1. temperaturethe mixture was heated
2. temperatureunder reflux for 2 h
3. temperatureUpon cooling the pH of the solution
4. filtrationThe solid was filtered off
5. washwashed with water
6. customdried