Hydrochloric Acid → HCID 131716988, compound

Participants

Reaction Steps

Under argon to a solution of 2-tertbutoxycarbonylamino-1,2-dihydro-3(4H) -phenanthrenone (74 mg) in anhydrous diethyl ether (5 ml) was added a saturated solution of hydrochloric acid in diethyl ether (5 ml). The mixture was stirred for 6 hours and the formed precipitate was filtered and dried under vacuum to afford the title compound as a white solid (42 mg)

Provenance & Evidence