Hydrochloric Acid → HCID 131716988, compound

HRID 1030644Notes

Reaction equation

HRID 1030644 reaction equation
C(OC([NH:8][CH:9]1[C:22](=[O:23])[CH2:21][C:20]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]=[CH:12][C:11]=2[CH2:10]1)=O)(C)(C)C.[ClH:24]>C(OCC)C>[ClH:24].[NH2:8][CH:9]1[C:22](=[O:23])[CH2:21][C:20]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH:13]=[CH:12][C:11]=2[CH2:10]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 19995578HCID 19995578, compound

Product 1

HCID 131716988HCID 131716988, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

Under argon to a solution of 2-tertbutoxycarbonylamino-1,2-dihydro-3(4H) -phenanthrenone (74 mg) in anhydrous diethyl ether (5 ml) was added a saturated solution of hydrochloric acid in diethyl ether (5 ml). The mixture was stirred for 6 hours and the formed precipitate was filtered and dried under vacuum to afford the title compound as a white solid (42 mg)

Workup

  1. filtrationthe formed precipitate was filtered
  2. customdried under vacuum

Sources & evidence

ORD record
ord-62e27c27e7864653af6235ece57c94a7
Source dataset
uspto-grants-1992_04
Patent number
US05106861

Reaction notes

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