HRID1030814

反应详情

EQUATION

反应方程式

HRID 1030814 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

5.80 g of the 4-dodecyl-2-nitrophenol obtained in (2) above was mixed with 500 mg of 5% active carbon-supported palladium, and 150 ml of tetrahydrofuran and the resulting mixture was contacted with hydrogen at room temperature for 7 hours to reduce the nitro group. The reaction mixture was filtered, and then the solvent was distilled off to obtain 5.21 g of 4-dodecyl-2-aminophenol.

WORKUP

后处理

  1. additionabove was mixed with 500 mg of 5% active carbon-
  2. filtrationThe reaction mixture was filtered
  3. distillationthe solvent was distilled off