HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 19025387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | p-Ethoxyphenyl isothiocyanate | HCID 77006 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19025387 | HCID 19025387 | 79.5% |
Reaction Steps
Following procedures similar to those employed in Step A of Example 2, the reaction of 2.5 g (0.0698 mole) of 4-ethoxyphenyl isothiocyanate and 3.22 g (0.0698 mole) of methylhydrazine in 100 ml of ethanol yielded 12.5 g of 4-(4-ethoxyphenyl)-2-methyl-3-thiosemicarbazide as a solid. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05108486 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-7350fbacbfcc40959fdb960bbc440c53 |
| Source note | uspto-grants-1992_04 |