HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 14460365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 14460323 | HCID 14460323 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14460365 | HCID 14460365 | — |
Reaction Steps
286 μl of a solution of chlorine in carbon tetrachloride containing 1.14 g/10 ml is added at -60° C. to a solution of 110 mg of p-nitrobenzyl 5-azido-2-(4-tert-butylthio-2-oxo-1-azetidinyl)-4,4-dimethyl-3-oxopentanoate in 9 ml of methylene chloride. The reaction solution is evaporated in a rotary evaporator, 119 mg of yellow oil being obtained. IR spectrum in CH2Cl2 : 2930, 2860, 2105, 1780, 1755, 1720, 1610, 1530, 1350, 1190 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05108747 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-046ad0bb02bb433b86cb7ecdad8de9da |
| Source note | uspto-grants-1992_04 |