HRID1031061

反应详情

EQUATION

反应方程式

HRID 1031061 的结构方程式

PROCEDURE

实验过程

Analogously to Example 7a), from 50 g. 2-methyl-4-nitroaniline is prepared 81.3 g. (88% of theory) N-benzyloxycarbonyl-2-methyl-4-nitroaniline which is reduced with sodium dithionite to give 44 g. 4-benzyloxycarbonylamido-3-methylaniline; m.p. 60°-62° C.

WORKUP

后处理

  1. customto give 44 g