HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 2-(N-methyl-N-(methoxycarbonyl)amino)-4'-propoxyacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-(N-methyl-N-(methoxycarbonyl)amino)-4'-difluoromethoxyacetophenone | HCID 18980988 | — |
| Product | 2-(N-methyl-N-(methoxycarbonyl)amino)-4'-propoxyacetophenone | HCID 19786521 | — |
Reaction Steps
By substantially following the procedure given in Example 19b, substituting 2-(N-methyl-N-(methoxycarbonyl)amino)-4'-propoxyacetophenone for 2-(N-methyl-N-(methoxycarbonyl)amino)-4'-difluoromethoxyacetophenone and using diethyl ether as solvent and continuing with Example 19dii the expected compound, an oil, bp 150°-160° C. at 0.2 torr, was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05109014 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-be85aa39c7c34273b5ee1e085c23ba7b |
| Source note | uspto-grants-1992_04 |