Anthranilic Acid → HCID 362691, compound

HRID 1031293Notes

Reaction equation

HRID 1031293 reaction equation
Nc1ccccc1C(=O)O.O=[N+]([O-])c1ccc(S(=O)(=O)Cl)cc1>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>O=C(O)c1ccccc1NS(=O)(=O)c1ccc([N+](=O)[O-])cc1

Participants

7

Reactant 2

HCID 227Anthranilic AcidHCID 74044-Nitrobenzenesulfonyl chloride

Product 1

HCID 362691HCID 362691, compoundYield 89%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-6a159be3b3874798b538af3b44c8a7be
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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