4-Nitrobenzenesulfonyl chloride → HCID 1713069, compound

HRID 1031296Notes

Reaction equation

HRID 1031296 reaction equation
CCOC(=O)CN.O=[N+]([O-])c1ccc(S(=O)(=O)Cl)cc1>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>CCOC(=O)CNS(=O)(=O)c1ccc([N+](=O)[O-])cc1

Participants

7

Reactant 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 12176Glycine ethyl ester

Product 1

HCID 1713069HCID 1713069, compoundYield 97%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-bd879f30d24f4d42b175fe559e3c9ce5
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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