Anthranilic Acid → HCID 2329216, compound

HRID 1031304Notes

Reaction equation

HRID 1031304 reaction equation
COc1ccc(S(=O)(=O)Cl)cc1OC.Nc1ccccc1C(=O)O>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>COc1ccc(S(=O)(=O)Nc2ccccc2C(=O)O)cc1OC

Participants

7

Reactant 2

HCID 227Anthranilic AcidHCID 27341833,4-Dimethoxybenzenesulfonyl chloride

Product 1

HCID 2329216HCID 2329216, compoundYield 85%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-967ac60e6bb843d7b9d6a50e7ea93962
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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