Methyl 4-aminobutanoate → HCID 3668631, compound

HRID 1031307Notes

Reaction equation

HRID 1031307 reaction equation
COC(=O)CCCN.COc1ccc(S(=O)(=O)Cl)cc1OC>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>COC(=O)CCCNS(=O)(=O)c1ccc(OC)c(OC)c1

Participants

7

Reactant 2

HCID 18614Methyl 4-aminobutanoateHCID 27341833,4-Dimethoxybenzenesulfonyl chloride

Product 1

HCID 3668631HCID 3668631, compoundYield 90%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-fd989edc957840599955fbf9a02cabb0
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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