2-Pentanamine → HCID 2886792, compound

HRID 1031308Notes

Reaction equation

HRID 1031308 reaction equation
CCCC(C)N.Cc1cc(C)c(S(=O)(=O)Cl)c(C)c1>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>CCCC(C)NS(=O)(=O)c1c(C)cc(C)cc1C

Participants

7

Reactant 2

HCID 122462-PentanamineHCID 130462-Mesitylenesulfonyl chloride

Product 1

HCID 2886792HCID 2886792, compoundYield 85%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-04df145abead4a48977c3a7e32cc698e
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

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