P-Anisidine → HCID 669057, compound

HRID 1031311Notes

Reaction equation

HRID 1031311 reaction equation
COc1ccc(N)cc1.Cc1cc(C)c(S(=O)(=O)Cl)c(C)c1>CC(C)=O.O.O=C([O-])O.OCCOCCOCCOCCOCCO.[Na+]>COc1ccc(NS(=O)(=O)c2c(C)cc(C)cc2C)cc1

Participants

7

Reactant 2

HCID 7732P-AnisidineHCID 130462-Mesitylenesulfonyl chloride

Product 1

HCID 669057HCID 669057, compoundYield 100%

Reagents, catalysts & solvents 4

HCID 516892Sodium BicarbonateReagentHCID 180AcetoneSolventHCID 962WaterSolventHCID 62551Pentaethylene glycolSolvent

Conditions

Temperature
25 °C

Workup

  1. additionNo procedure recorded
  2. extractionKeep organic
  3. washNo procedure recorded
  4. washNo procedure recorded
  5. dry with materialNo procedure recorded
  6. concentrationNo procedure recorded

Sources & evidence

ORD record
ord-c2e5e7fa7a224532a21ec3ae2bd99098
Source dataset
39 compound library from "Building a Sulfonamide Library by Eco-Friendly Flow Synthesis"
Original link
View source

Reaction notes

Loading…