HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrophenol → 2-(3-Chloro-5-trifluoromethyl-2-pyridyloxy)nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrophenol | HCID 6947 | — |
| Reactant | 3-Chloro-2-fluoro-5-(trifluoromethyl)pyridine | HCID 1268075 | — |
| Product | 2-(3-Chloro-5-trifluoromethyl-2-pyridyloxy)nitrobenzene | HCID 15017530 | 63% |
Reaction Steps
This material was prepared in 63% yield from 3-chloro-2-fluoro-5-trifluoromethylpyridine and 2-nitrophenol following the general procedure outlined in Example 104. The product was isolated as an amber oil which was characterized by IR and 1H NMR spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954163 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-1ca131e423954e45b30491b0ee95ba16 |
| Source note | uspto-grants-1990_09 |