HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14459491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-3-Bromopropylphthalimide | HCID 21611 | — |
| Reactant | HCID 14459461 | HCID 14459461 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14459491 | HCID 14459491 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
A mixture of 3.16 g (10 mmol) of 5-methyl-6-[3-nitro-4-(1-piperazinyl)-phenyl]-4,5-dihydro-3(2H)-pyridazinone, 2.68 g (10 mmol) of N-(3-bromopropyl)-phthalimide, 1.38 g (10 mmol) of potassium carbonate and 50 ml of dimethyl formamide is stirred at 100° C. for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954501 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-fd0cd19d0cd0409484003116fe1d4d4a |
| Source note | uspto-grants-1990_09 |