Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → HCID 53937148, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Phosphonic acid, [2-(4-morpholinyl)-2-oxoethyl]-, diethyl ester | HCID 11207805 | — |
| 반응물 | HCID 14878865 | HCID 14878865 | — |
| 생성물 | HCID 53937148 | HCID 53937148 | 32.1% |
반응 단계
In the same manner as in Example 1, using 5-(3,4-dimethoxybenzoyl)-2-(N-methylanilino)pyridine (500 mg), diethylphosphonoacetic acid morpholide (800 mg) and 60% sodium hydride (150 mg), E-isomer (250 mg) and Z-isomer (212 mg) of 4-[3-(2-(N-methylanilino)-5-pyridyl)-3-(3,4-dimethoxyphenyl)acryloyl]morpholine (Compound No.62) were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04954497 |
| 출처 데이터셋 | uspto-grants-1990_09 |
| ORD ID | ord-60040d8caa1041c58f900df3b01c3d8d |
| 출처 메모 | uspto-grants-1990_09 |