HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22168011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3,4-Dichlorophenylacetic acid | HCID 79874 | — |
| Reactant | HCID 22168045 | HCID 22168045 | — |
| Reactant | HCID 22168074 | HCID 22168074 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22168011 | HCID 22168011 | — |
Reaction Steps
Prepared as Ex. No. 5, from 13.2 g (33.50 mmoles) of a mixture containing 1-(pyrrolidin-1-yl)methyl-8-hydroxy-1,2,3,4-tetrahydroisoquinoline dihydrobromide and 1-(pyrrolidin-1-yl)methyl-6-hydroxy-1,2,3,4-tetrahydroisoquinoline dihydrobromide, 9.6 g (46.8 mmoles) of 3,4-dichlorophenylacetic acid, 14 ml (99.6 mmoles) of triethylamine and 17 g (82.52 mmoles) of dicyclohexylcarbodiimide, in 280 ml of dry chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954509 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-e1d936a93b404b44b7d7897a233d757b |
| Source note | uspto-grants-1990_09 |