HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 67869533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3,4-Dichlorophenylacetic acid | HCID 79874 | — |
| Reactant | HCID 21274546 | HCID 21274546 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67869533 | HCID 67869533 | — |
Reaction Steps
Prepared as Ex. No. 1, from 2.7 g (13.30 mmoles) of 1- dimethylamino-eth-1-yl-1,2,3,4-tetrahydroisoquinoline (diastereoisomeric mixture), 3.05 g (15.00 mmoles) of 3,4-dichlorophenylacetic acid and 4.2 g (20.39 mmoles) of dicyclohexylcarbodiimide, in 100 ml of dry methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954509 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-8eeb33b8cff641c4a2de495b77baf8a5 |
| Source note | uspto-grants-1990_09 |