HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3,4-Dichlorophenyl)acetyl chloride → HCID 22168097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3,4-Dichlorophenyl)acetyl chloride | HCID 2758149 | — |
| Reactant | HCID 15005446 | HCID 15005446 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22168097 | HCID 22168097 | 105.7% |
Reaction Steps
Prepared as Ex. No. 33, from 1.3 g (4.71 mmoles) of 1-(pyrrolidin-1-yl)methyl-5,6-dimethoxy-1,2,3,4-tetrahydroisoquinoline and 1.1 g (4.92 mmoles) of 3,4-dichlorophenyl acetyl chloride in 40 ml of dry chloroform. The crude product was crystallized from 40 ml of ethyl acetate, to yield 1.3 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04954509 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-5d58168a7ff94930ae6226608b0e1234 |
| Source note | uspto-grants-1990_09 |