Methyl iodide → HCID 14722469, compound

HRID 1031738Notes

Reaction equation

HRID 1031738 reaction equation
[CH3:1][S:2]([NH:5][C:6]1[C:16]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:15][C:9]2[C:10](=[O:14])[CH:11]=[CH:12][O:13][C:8]=2[CH:7]=1)(=[O:4])=[O:3].[CH3:24]I.[H-].[Na+]>>[CH3:24][N:5]([C:6]1[C:16]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:15][C:9]2[C:10](=[O:14])[CH:11]=[CH:12][O:13][C:8]=2[CH:7]=1)[S:2]([CH3:1])(=[O:3])=[O:4]

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 24758Sodium hydrideHCID 106164807-methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one

Product 1

HCID 14722469HCID 14722469, compound

Procedure

7-Methylsulfonylamino-6-phenoxy-4H-1-benzopyran-4-one was reacted with methyl iodide in the presence of sodium hydride to obtain 7-(N-methyl-N-methylsulfonylamino)-6-phenoxy-4H-1-benzopyran-4-one.

Sources & evidence

ORD record
ord-21c19dc68244490ebb313f5167b310fe
Source dataset
uspto-grants-1990_09
Patent number
US04954518

Reaction notes

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