HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 14421320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 105950-89-8 | HCID 14306130 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14421320 | HCID 14421320 | — |
Reaction Steps
A solution of 12 g of 2-methoxymethyl-4-chloropyrimidine and 15 ml of morpholine in 50 ml of dichloromethane was stirred at room temperature for 3 hours. The reaction solution was washed several times with water. The organic phase was dried and, after purification by column chromatography, yielded 13 g of 2-methoxymethyl4-morpholinopyrimidine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04956366 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-2f69a80f6c1345c985a5b9f9eb515549 |
| Source note | uspto-grants-1990_09 |