HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromopinacolone → HCID 178488981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | HCID 54562755 | HCID 54562755 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178488981 | HCID 178488981 | — |
Reaction Steps
A solution of 160 mg of 1-[[p-(dimethylamino)benzylidene]amino]-2-(p-methoxyphenyl)imidazole and 400 mg of 1-bromo-3,3-dimethyl-2-butanone in 3 ml of acetonitrile is stirred at 60° for 20 hours. The product is removed by filtration and washed with ether. There is obtained 1-[[p-(dimethylamino)benzylidene]amino]-2-(p-methoxyphenyl)-3-(pivaloylmethyl)imidazolium bromide of melting point 262°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04956470 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-6a0e47cf24e343e1bb92808ea8e8bd32 |
| Source note | uspto-grants-1990_09 |