HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 14796243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 21924318 | HCID 21924318 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14796243 | HCID 14796243 | — |
Reaction Steps
A solution of 2-(2-chlorophenyl)maleimide (4.70 g) and aniline (3.069) in ethanol (50 ml) is refluxed for 38 hours. The reaction mixture is concentrated and the residue is subjected to silica gel chromatography, with elution being carried out with n-hexane-ethyl acetate (4:1-1:1) to give 2-(2-chlorophenyl)-3-anilinosuccinimide (oil) (3.71 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957537 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-dd0820b6479c42e990c085a68d480679 |
| Source note | uspto-grants-1990_09 |