HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 69553959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | 4-(Trifluoromethyl)benzaldehyde | HCID 67996 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 69553959 | HCID 69553959 | — |
Reaction Steps
Methylamine was passed into a solution of about 10.1 g of 4-(trifluoromethyl)benzaldehyde in about 100 ml of benzene over MgSO4 for four hours with stirring. The solution was filtered, and then the solvent was evaporated to give N-[4-(trifluoromethyl)benzylidene]methylamine as an oil. This was taken up in benzene and catalytically (5% Pd/C) hydrogenated to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957533 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-70e7249dd32048f3900a3f09cd74f261 |
| Source note | uspto-grants-1990_09 |