HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → (5 Chlorobenzoxazol-2-yl methyl)triphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 2-(Bromomethyl)-5-chlorobenzo[d]oxazole | HCID 12745945 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | (5 Chlorobenzoxazol-2-yl methyl)triphenylphosphonium bromide | HCID 23055263 | — |
Reaction Steps
A solution of the bromide (500 mg) (Step 3) and triphenylphosphine (740 mg) in CH3CN (5 mL) was stirred at room temperature overnight. The reaction mixture was diluted with Et2O (20 mL), stirred for 30 min, and filtered to give the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957932 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-07367f49a302496b9fb474ee9f3acff1 |
| Source note | uspto-grants-1990_09 |