HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14556315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Bromo-2-[bis(4-fluorophenyl)methoxy]ethane | HCID 10568186 | — |
| Reactant | HCID 14556324 | HCID 14556324 | — |
| Product | HCID 14556315 | HCID 14556315 | 73% |
Reaction Steps
Proceeding as in Example 9, using 16.4 g (50 mmole) of 1-[bis(4-fluorophenyl)methoxy]-2-bromoethane, 10.3 g (50 mmole) of 3-(3-1isopropoxyphenyl)pyrrolidine and 13.8 g (100 mmole) of potassium carbonate, there was obtained after silica gel column filtration, 16.4 g (yield: 73%) of 1-[2-[bis(4-fluorophenyl) methoxy]ethyl]-3-(3-isopropoxyphenyl)pyrrolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957927 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-3ba46551880346929a4ba720c50f4b79 |
| Source note | uspto-grants-1990_09 |