huagongshe.com
HRID1032340

反应详情

EQUATION

反应方程式

HRID 1032340 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Fc1ccc(C(OCCBr)c2ccc(F)cc2)cc1
HCID10568186

Benzene, 1,1'-[(2-bromoethoxy)methylene]bis[4-fluoro-

C15H13BrF2O

结构：CC(C)Oc1cccc(C2CCNC2)c1
HCID14556324

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Oc1cccc(C2CCN(CCOC(c3ccc(F)cc3)c3ccc(F)cc3)C2)c1
HCID14556315

未命名化合物

收率 73%

PROCEDURE

实验过程

Proceeding as in Example 9, using 16.4 g (50 mmole) of 1-[bis(4-fluorophenyl)methoxy]-2-bromoethane, 10.3 g (50 mmole) of 3-(3-1isopropoxyphenyl)pyrrolidine and 13.8 g (100 mmole) of potassium carbonate, there was obtained after silica gel column filtration, 16.4 g (yield: 73%) of 1-[2-[bis(4-fluorophenyl) methoxy]ethyl]-3-(3-isopropoxyphenyl)pyrrolidine.

WORKUP

后处理

  1. customthere was obtained