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HRID1032342

反应详情

EQUATION

反应方程式

HRID 1032342 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COc1cccc(C2CCCN2)c1
HCID3613824

2-(3-methoxyphenyl)pyrrolidine

C11H15NO

结构：Fc1ccc(C(OCCBr)c2ccc(F)cc2)cc1
HCID10568186

Benzene, 1,1'-[(2-bromoethoxy)methylene]bis[4-fluoro-

C15H13BrF2O

PRODUCTS

生成物

1
结构：COc1cccc(C2CCCN2CCOC(c2ccc(F)cc2)c2ccc(F)cc2)c1
HCID14556317

未命名化合物

收率 52%

PROCEDURE

实验过程

Proceeding as in Example 9, using 9.8 g (30 mmole) of 1-[bis(4-fluorophenyl)methoxy]-2-bromoethane, 5.3 g (30 mmole) of (2-(3-methoxyphenyl)pyrrolidine and 8.3 g (60 mmole) of potassium carbonate, there was obtained after silica gel column filtration, 6.7 g (yield: 52%) of 1-[2-[bis(4-fluorophenyl)methoxy]ethyl]-2-(3-methoxyphenyl)pyrrolidine.

WORKUP

后处理

  1. customthere was obtained