HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14556317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(3-Methoxyphenyl)pyrrolidine | HCID 3613824 | — |
| Reactant | 1-Bromo-2-[bis(4-fluorophenyl)methoxy]ethane | HCID 10568186 | — |
| Product | HCID 14556317 | HCID 14556317 | 52% |
Reaction Steps
Proceeding as in Example 9, using 9.8 g (30 mmole) of 1-[bis(4-fluorophenyl)methoxy]-2-bromoethane, 5.3 g (30 mmole) of (2-(3-methoxyphenyl)pyrrolidine and 8.3 g (60 mmole) of potassium carbonate, there was obtained after silica gel column filtration, 6.7 g (yield: 52%) of 1-[2-[bis(4-fluorophenyl)methoxy]ethyl]-2-(3-methoxyphenyl)pyrrolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957927 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-54d5a1f10e0848908615873d78167e69 |
| Source note | uspto-grants-1990_09 |