HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → (Diphenylmethoxy) acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzhydryloxyacetic acid | HCID 597513 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | (Diphenylmethoxy) acetyl chloride | HCID 13111194 | 73% |
Reaction Steps
8.1 g (68.1 mmole) of thionyl chloride was added to a solution of 5.5 g (22.7 mmole) of (diphenylmethoxy) acetic acid in 150 cm3 of benzene. The solution was refluxed for 5 hours, then evaporated to dryness under reduced pressure. Distillation of the residue yielded 4.3 g (yield: 73%) of (diphenylmethoxy) acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957927 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-522973b92c3346e4b8cedce66aaf0cba |
| Source note | uspto-grants-1990_09 |