HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 14838405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Chroman-3-ylmethanamine | HCID 4962852 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14838405 | HCID 14838405 | 95% |
Reaction Steps
3.03 g (35.2 mmol) of acrylic acid methyl ester are added to a solution of 2.61 g (16 mmol) of 3-aminomethylchroman in 20 ml of methanol. The reaction solution is stirred for 16 hours at 50° and, after cooling, is concentrated by evaporation in vacuo. 5.1 g (95%) of N,N-bis(2-methoxycarbonylethyl)-N-(chroman-3-ylmethyl)-amine are obtained in the form of a reddish oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04957928 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-3f512efba59440a09deb72bc63c4b683 |
| Source note | uspto-grants-1990_09 |