反应详情

590 mg (2.44 mmol) of N-benzyl-5,6-dihydroxyisoindoline was dissolved in 10 ml of acetone, and 0.16 ml (2.5 mmol) of methyl iodide was added thereto at room temperature. The mixture was left to stand for 4 hours, and the precipitated crystals were collected by filtration and washed with 10 ml of acetone to obtain 733 mg of the above identified compound.

1. customat room temperature
2. waitThe mixture was left
3. filtrationthe precipitated crystals were collected by filtration
4. washwashed with 10 ml of acetone
5. customto obtain 733 mg of the