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HRID1032527

反应详情

EQUATION

反应方程式

HRID 1032527 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(C)ccc1[N+](=O)[O-]
HCID97455

5-Methyl-2-nitroanisole

C8H9NO3

结构：CC1CCC(C(C)C)C(N(C2CC(C)CCC2C(C)C)C(OC(C)(C)C)N(C2CC(C)CCC2C(C)C)C2CC(C)CCC2C(C)C)C1
HCID22165996

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(C=CN(C)C)ccc1[N+](=O)[O-]
HCID54285175

未命名化合物

PROCEDURE

实验过程

83.5 of 5-methyl-2-nitroanisole and 162.0 g of tert-butoxybis(dimenthylamino)methane is heated for 8 hours to 100° C. After cooling, 111.0 g of N,N-dimenthyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine is crystallized, mp 57°-58.5° C.

WORKUP

后处理

  1. temperatureAfter cooling
  2. custom111.0 g of N,N-dimenthyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine is crystallized