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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1032527Generated: October 25, 2026

5-Methyl-2-nitroanisole → N,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine

https://huagongshe.com/reaction/1032527

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Methyl-2-nitroanisoleHCID 97455—
ReactantTert-butoxybis(dimenthylamino)methaneHCID 22165996—
ProductN,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amineHCID 54285175—

Reaction Steps

83.5 of 5-methyl-2-nitroanisole and 162.0 g of tert-butoxybis(dimenthylamino)methane is heated for 8 hours to 100° C. After cooling, 111.0 g of N,N-dimenthyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine is crystallized, mp 57°-58.5° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04958026
Source datasetuspto-grants-1990_09
ORD IDord-1825ee651313439b907e49781a3f0326
Source noteuspto-grants-1990_09