HRID1032536

反应详情

EQUATION

反应方程式

HRID 1032536 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In the presence of 100 mg of palladiumcarbon, 2.6 g of 5-(2-aminoethyl)-2-benzyloxyaniline, hydrochloride, is hydrogenated in 20 ml of methanol; after recrystallization from ethanol, 0.52 g of 5-(2-aminoethyl)-2-hydroxyaniline, hydrochloride, is obtained, mp 159°-164° C.

WORKUP

后处理

  1. customafter recrystallization from ethanol, 0.52 g of 5-(2-aminoethyl)-2-hydroxyaniline, hydrochloride
  2. customis obtained