HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Aminoethyl)-2-benzyloxyaniline, hydrochloride → 5-(2-Aminoethyl)-2-hydroxyaniline, Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Aminoethyl)-2-benzyloxyaniline, hydrochloride | HCID 131716571 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-(2-Aminoethyl)-2-hydroxyaniline, Hydrochloride | HCID 131716570 | — |
Reaction Steps
In the presence of 100 mg of palladiumcarbon, 2.6 g of 5-(2-aminoethyl)-2-benzyloxyaniline, hydrochloride, is hydrogenated in 20 ml of methanol; after recrystallization from ethanol, 0.52 g of 5-(2-aminoethyl)-2-hydroxyaniline, hydrochloride, is obtained, mp 159°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04958026 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-672bb09c633c4a55a30d99b3f4409103 |
| Source note | uspto-grants-1990_09 |