HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86744232, compound → HCID 86744231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86744232 | HCID 86744232 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86744231 | HCID 86744231 | — |
Reaction Steps
A solution of N,N-bis-(4-nitrophenethyl)methylamine (1.2 g, 3.6 mmol) in ethanol (50 ml) containing 5% Pd/C (0.15 g) was stirred under a hydrogen atmosphere (50 p.s.i.) for 4 hours. The reaction mixture was filtered and the solvent evaporated to give the title compound as an oil, yield 1.0 g, which was used directly without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04959366 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-4a767b3e472a4fbc9c93ad05a0f97f28 |
| Source note | uspto-grants-1990_09 |