HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178470072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Ethyl-1,4-dihydro-4-oxo-7-(3-pyridinyl)-3-quinolinecarboxylic acid | HCID 10447150 | — |
| Reactant | HCID 178470078 | HCID 178470078 | — |
| Product | HCID 178470072 | HCID 178470072 | — |
Reaction Steps
Ethyl 1,4-dihydro-2-hydroxy-1-methyl-4-oxo-7-(4-pyridinyl)-3-quinolinecarboxylate was prepared from 7.20 g dioxobenzoxazine of Example 38, part (a), 1.66 g 60% sodium hydride and 1.95 ml methyl iodide according to the procedure of Example 38, part (b), and was obtained (4.50 g) as a yellow solid, m.p. about 184° C(decompn.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04959363 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-80e0f111516e420bb86cf3aadae7756f |
| Source note | uspto-grants-1990_09 |