HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycolaldehyde → HCID 10040359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycolaldehyde | HCID 756 | — |
| Reactant | Imidazole | HCID 795 | — |
| Reactant | tert-Butyldiphenylchlorosilane | HCID 94078 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10040359 | HCID 10040359 | — |
Reaction Steps
In the manner described in Example 14c, 5.15 g of glycolaldehyde and 26.78 ml of tert-butyldiphenylchlorosilane were reacted in the presence of 7.61 g of imidazole and 26 ml of absolute dimethylformamide whereby after column chromatography with ether/petroleum ether (1:2) 21.26 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04959391 |
| Source dataset | uspto-grants-1990_09 |
| ORD ID | ord-0a8968fd164c437188ac0cf1d4af3f41 |
| Source note | uspto-grants-1990_09 |