Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 10363611 | HCID 10363611 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10357226 | HCID 10357226 | 73.1% |
Reaction Steps
A suspension of 2-(diaminomethyleneamino)-4-[5-{3-(benzoyl)thioureido}methylfuran-2-yl]thiazole (3.20 g) and sodium hydroxide (0.32 g) in methanol (30 ml) was stirred at 60° C. for one hour. The reaction mixture was cooled in an ice bath and the resulting precipitate was collected by filtration and washed with methanol to afford 2-(diaminomethyleneamino)-4-(5-thioureidomethylfuran-2-yl)thiazole (1.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05308857 |
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| Source dataset | uspto-grants-1994_05 |
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| ORD ID | ord-ba87d4c5274049688b601b5efe5265f9 |
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| Source note | uspto-grants-1994_05 |
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