HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetone → HCID 10088260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | HCID 10357226 | HCID 10357226 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10088260 | HCID 10088260 | 83.6% |
Reaction Steps
A suspension of 2-(diaminomethyleneamino)-4-(5-thioureidomethylfuran-2-yl)thiazole (0.70 g) and chloroacetone (0.22 g) in ethanol (15 ml) was refluxed for 4 hours with stirring. The solvent was evaporated in vacuo and the residue was recrystallized from a mixture of methanol and diisopropyl ether to afford 2-(diaminomethyleneamino)-4-[5-(4-methylthiazol-2-yl)aminomethylfuran-2-yl]thiazole (0.66 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05308857 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-814beca9a260499384c0a3b768d976da |
| Source note | uspto-grants-1994_05 |