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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1033053Generated: October 31, 2026

Chloroacetone → HCID 10088260, compound

https://huagongshe.com/reaction/1033053

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChloroacetoneHCID 6571—
ReactantHCID 10357226HCID 10357226—
SolventEthanolHCID 702—
ProductHCID 10088260HCID 1008826083.6%

Reaction Steps

A suspension of 2-(diaminomethyleneamino)-4-(5-thioureidomethylfuran-2-yl)thiazole (0.70 g) and chloroacetone (0.22 g) in ethanol (15 ml) was refluxed for 4 hours with stirring. The solvent was evaporated in vacuo and the residue was recrystallized from a mixture of methanol and diisopropyl ether to afford 2-(diaminomethyleneamino)-4-[5-(4-methylthiazol-2-yl)aminomethylfuran-2-yl]thiazole (0.66 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05308857
Source datasetuspto-grants-1994_05
ORD IDord-814beca9a260499384c0a3b768d976da
Source noteuspto-grants-1994_05