HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67826748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67826411 | HCID 67826411 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67826748 | HCID 67826748 | 5.8% |
Reaction Steps
A mixture of compound from Step A (100 mg., 0.42 mM) CH3OH (25 ml.) and 12N HCl (3 ml.) was heated at reflux for 24 hours. The CH3OH was evaporated in vacuo. The aqueous phase was made basic with saturated sodium carbonate, evaporated to dryness and extracted with hot ethyl acetate which was evaporated to dryness to give 5 mg of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05308863 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-fb6d694a3f94478a8e53143200920eb9 |
| Source note | uspto-grants-1994_05 |