HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 4418042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Product | HCID 4418042 | HCID 4418042 | — |
Reaction Steps
Following Intermediate Method 5, the reaction of 2-chloro-5-nitropyridine, (XXII) with diethylamine produces 2-diethylamino-5-nitropyridine, (XXII). The reduction of this compound (XXII) with iron powder in aqueous hydrochloric acid and ethanol yields 5-amino-2-diethylaminopyridine, (XXIII).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310724 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-93650fbb3a1b4ba5a55583b70df0acb0 |
| Source note | uspto-grants-1994_05 |