HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 19025443, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 19025453 | HCID 19025453 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19025443 | HCID 19025443 | 98.3% |
Reaction Steps
Following procedures similar to those employed in Step A of Example 2, the reaction of 2.9 g (0.012 mole) of 4-diethylamino-2,5-difluorophenyl isothiocyanate with 0.55 g (0.012 mole) of methylhydrazine in 75 ml of ethanol yielded 3.4 g of 4-(4-diethylamino-2,5-difluorophenyl) -2-methyl-3-thiosemicarbazide. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310724 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-aefd716ee15348ffae301746c4e9bdd0 |
| Source note | uspto-grants-1994_05 |