Phenol → HCID 67848231, compound

HRID 1033263Notes

Reaction equation

HRID 1033263 reaction equation
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>CC(C)=O>[NH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1.[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 996PhenolHCID 8082Piperidine

Product 1

HCID 67848231HCID 67848231, compoundYield 94.8%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

To a solution of 9.4 g (0.1 mol) of phenol dissolved in 100 ml of acetone, 8.5 g (0.1 mol) of piperidine was added dropwise under stirring, and the precipitated crystals were filtered and dried, to obtain a 17.0 g (yield 55.0%) of phenol piperidine salt (molar ratio 1:1) of white crystals.

Workup

  1. filtrationthe precipitated crystals were filtered
  2. customdried

Sources & evidence

ORD record
ord-c1b42e2fb93b4d28b99b58852585968b
Source dataset
uspto-grants-1994_05
Patent number
US05310818

Reaction notes

Loading…