HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-((tert-Butoxycarbonyl)amino)hexanoic acid → HCID 19025520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-((tert-Butoxycarbonyl)amino)hexanoic acid | HCID 637602 | — |
| Reactant | 3-Amino-2,3,4,5-tetrahydro-1H-benzazepin-2-one | HCID 4434433 | — |
| Product | HCID 19025520 | HCID 19025520 | — |
Reaction Steps
Prepared from 6-(t-butoxycarbonylamino)hexanoic acid and 3-amino-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one (Example 1, Step A) by the procedure described in Example 25, Step A. 1H NMR (200 MHz, CDCl3): 1.2-1.7 (m,14 H), 1.92 (m,2 H), 2.16 (t,5 Hz,1 H), 2.5-3.1 (m,6 H), 4.53 (m,2 H), 6.54 (d,7 Hz,1 H), 6.96 (m,1 H), 7.18 (m,3 H), 8.00 (s,1 H). FAB-MS: calculated for C21H31N3O4 389; found 390 (M+H,18%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310737 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-7dd8a6e9cc8248fa8d8eaa3598004c30 |
| Source note | uspto-grants-1994_05 |