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HRID1033381

反应详情

EQUATION

反应方程式

HRID 1033381 的结构方程式

REACTANTS

反应物

2
结构：NC1CCc2ccccc2NC1=O
HCID4434433

3-Amino-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one

C10H12N2O

结构：CC(C)(C)OC(=O)N(C(=O)OC(C)(C)C)[C@@H](CCCCN)C(=O)O
HCID22792075

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCCC[C@H](NC(=O)OC(C)(C)C)C(=O)NC1CCc2ccccc2NC1=O
HCID18651402

未命名化合物

PROCEDURE

实验过程

Prepared from Na, Ne -di(t-butoxycarbonyl)L-lysine and 3-amino-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one (Example 1, Step A) by the procedure described in Example 25, Step A. 1H NMR (200 MHz, CDCl3): 1.2-2.1 (m,24 H), 2.6-3.3 (m,6 H), 4.20 (m,1 H), 4.62 (m,2H), 5.26 (m,1H), 7.0-7.4 (m,4 H). FAB-MS: calculated for C26H40N4O6 504; found 505 (M+H,20%).