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HRID1033408

反应详情

EQUATION

反应方程式

HRID 1033408 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NC(C)(C)C(=O)O
HCID2733845

N-((1,1-Dimethylethoxy)carbonyl)-2-methyl-alanine

C9H17NO4

结构：N[C@@H]1CCc2ccccc2NC1=O
HCID10103689

(3R)-3-Amino-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one

C10H12N2O

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NC(C)(C)C(=O)N[C@@H]1CCc2ccccc2NC1=O
HCID10808566

未命名化合物

PROCEDURE

实验过程

Prepared from 2-(t-butoxycarbonylamino)-2-methylpropanoic acid and 3(R)-amino-2,3,4,5-tetrahydro-1H-[1]benzazepin-2-one (Example 1, Step B) by the procedure described in Example 1, Step F. 1H NMR (200MHz, CDCl3): 1.42 (s,12H), 1.46 (s,3H), 1.90 (m,1H), 2.5-3.0 (m,3H), 4.48 (m,1H), 5.01 (br s,1H), 6.97 (d,8Hz,1H), 7.1-7.3 (m,3H), 7.9 (br s,1H). FAB=MS: calculated for C19H27N3O4 361; found 362 (M+H,30%).